BS EN 13999-3-2009 Adhesives — Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application — Part 3 Determination of volatile aldehydes.pdf
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1、BRITISH STANDARD Adhesives Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application Part 3: Determination of volatile aldehydes ICS 83.180 ? BS EN 13999-3:2007 +A1:2009 This British Standard was published under the authority of the Standards
2、Policy and Strategy Committee on 31 May 2007 BSI 2009 ISBN 978 0 580 63986 9 National foreword BS EN 13999-3:2007+A1:2009 This British Standard is the UK implementation of EN 13999-3:2007+A1:2009. It supersedes BS EN 13999-3:2007 which is The start and finish of text introduced or altered by amendme
3、nt is indicated in the text by tags. Tags indicating changes to CEN text carry the number of CEN amendment. For example, text altered by CEN amendment A1 is indicated by ab. The UK participation in its preparation was entrusted to Technical Committee PRI/52, Adhesives. A list of organizations repres
4、ented on this committee can be obtained on request to its secretary. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard cannot confer immunity from legal obligations. withdrawn
5、. DateComments June 2009 Implementation of CEN amendment A1:2009 Amendments/corrigenda issued since publication the 30 EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 13999-3:2007+A1 April 2009 ICS 83.180Supersedes EN 13999-3:2007 English Version Adhesives - Short term method for measuring the
6、emission properties of low-solvent or solvent-free adhesives after application - Part 3: Determination of volatile aldehydes Adhsifs - Mthodes de mesurage rapide des caractristiques missives des adhsifs teneur faible ou nulle en solvants aprs application - Partie 3: Dosage des aldhydes volatiles Kle
7、bstoffe - Kurzzeit-Verfahren zum Messen der Emissionseigenschaften von lsemittelarmen oder lsemittelfreien Klebstoffen nach der Applikation - Teil 3: Bestimmung flchtiger Aldehyde This European Standard was approved by CEN on 8 March 2007 and includes Amendment 1 approved by CEN on 3 April 2009. CEN
8、 members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on appl
9、ication to the CEN Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the respons bility of a CEN member into its own language and notified to the CEN Management Centre
10、has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland,
11、Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2009 CEN All rights of exploitation in any form and by any m
12、eans reserved worldwide for CEN national Members. Ref. No. EN 13999-3:2007+A1:2009: E EN 13999-3:2007+A1:2009 (E) 2 Contents Page Foreword 3 SAFETY STATEMENT .4 1Scope 4 2Normative references 4 3Principle 4 4Reagents .5 5Apparatus .5 6Procedure .5 7Identification and calculation .7 8Interferences 8
13、9Precision and bias .8 10Test report 8 11Quality control 9 Bibliography . 10 BS EN 13999-3:2007+A1:2009 EN 13999-3:2007+A1:2009 (E) 3 Foreword This document (EN 13999-3:2007+A1:2009) has been prepared by Technical Committee CEN/TC 193 “Adhesives”, the secretariat of which is held by AENOR. This Euro
14、pean Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by October 2009, and conflicting national standards shall be withdrawn at the latest by October 2009. This document includes Amendment 1, approved by CEN on 200
15、9-04-03. This document supersedes !EN 13999-3:2007“. The start and finish of text introduced or altered by amendment is indicated in the text by tags ! “. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this Eu
16、ropean Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United K
17、ingdom. BS EN 13999-3:2007+A1:2009 ? ation on Bulgaria, Bulgaria, Iceland, Ire celand, Ire www.bzfxw.co Romania, Slo mania, Slo EN 13999-3:2007+A1:2009 (E) 4 SAFETY STATEMENT Persons using this European Standard should be familiar with the normal laboratory practice, if applicable. This Europea
18、n Standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate health and safety practices and to ensure compliance with any regulatory conditions. 1 Scope This European Standard specifies a procedure
19、for the determination of volatile aldehydes (especially formaldehyde and acetaldehyde) and other carbonyl compounds in the exhaust air of an emission test chamber after application of a low-solvent or solvent-free adhesive as defined in EN 923. The method is based on chemosorption of volatile carbon
20、yl compounds with 2,4-dinitrophenylhydrazine (in the following: DNPH) impregnated silica tubes or cartridges with subsequent solvent desorption, clean-up and liquid chromatographic analysis. The method permits measurement of several aldehydes including formaldehyde, acetaldehyde, propionaldehyde, bu
21、tyraldehyde, valeraldehyde, isovaleraldehyde, hexanal, benzaldehyde, 2,5-dimethylbenzaldehyde, o-tolualdehyde, m-tolualdehyde, p-tolualdehyde, crotonaldehyde in the concentration range of approximately 10 g/m to 1 mg/m (see ISO 16000-3). 2 Normative references The following referenced documents are
22、indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 1232, Workplace atmospheres Pumps for personal sampling of chemical agents Requiremen
23、ts and test methods EN 13999-1, Adhesives Short term method for measuring the emission properties of low-solvent or solvent- free adhesives after application Part 1: General procedure EN ISO 16000-9, Indoor air Part 9: Determination of the emission of volatile organic compounds from building product
24、s and furnishing Emission test chamber method (ISO 16000-9:2006) ISO 16000-3, Indoor air Part 3: Determination of formaldehyde and other carbonyl compounds Active sampling method 3 Principle A sufficient volume of test chamber air is drawn with an appropriate flow through silicagel tubes or cartridg
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