BS 1016-106.1.1-1996 ISO 609-1996.pdf
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1、BRITISH STANDARD BS 1016-106.1.1: 1996 ISO 609:1996 Methods for Analysis and testing of coal and coke Part 106: Ultimate analysis of coal and coke Section 106.1 Determination of carbon and hydrogen content Subsection 106.1.1 High temperature combustion method ICS 75.160.10 Licensed Copy: sheffieldun
2、 sheffieldun, na, Fri Nov 24 08:07:58 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS 1016-106.1.1:1996 This British Standard, having been prepared under the direction of the Sector Board for Materials and Chemicals, was published under the authority of the Standards Board and comes into effect on 15
3、October 1996 BSI 11-1998 The following BSI references relate to the work on this standard: Committee reference SFI/3 Draft for comment 93/508888 DC ISBN 0 580 26460 2 Committees responsible for this British Standard The preparation of this British Standard was entrusted to Technical Committee SFI/3,
4、 Analysis and testing of coal and coke, upon which the following bodies were represented: British Cement Association British Coal Corporation British Iron and Steel Producers Association Electricity Association GAMBICA (BEAMA Ltd.) Power Generation Contractors Association (PGCA (BEAMA Ltd.) Amendmen
5、ts issued since publication Amd. No.DateComments Licensed Copy: sheffieldun sheffieldun, na, Fri Nov 24 08:07:58 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS 1016-106.1.1:1996 BSI 11-1998i Contents Page Committees responsible Inside front cover National forewordii Introduction1 1Scope1 2Normative r
6、eferences1 3Principle1 4Reagents and materials1 5Apparatus2 6Preparation of the apparatus6 7Preparation of test sample6 8Procedure8 9Blank test8 10Expression of results8 11Precision9 12Test report9 Annex A (informative) Derivation of factors used in calculations in clause 1010 Figure 1 Typical tempe
7、rature-distribution curve for furnace3 Figure 2 Midvale tube4 Figure 3 Absorption train5 Figure 4 Arrangement of apparatus for the location of the silver gauze roll7 Table 19 Table A.110 Licensed Copy: sheffieldun sheffieldun, na, Fri Nov 24 08:07:58 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS 101
8、6-106.1.1:1996 ii BSI 11-1998 National foreword This British Standard has been prepared by SFI/3 and is identical to ISO 609:1996 Solid mineral fuels Determination of carbon and hydrogen High temperature combustion method, including Corrigendum 1:1996, both published by the International Organizatio
9、n for Standardization (ISO) and in the preparation of which the UK played a full part. BS 1016-106 will form a revision of Parts 6 to 11 of BS 1016. This Subsection supersedes the following: in BS 1016-6:1977, clauses 5 and 6 and that part of clause 11 relating to carbon and hydrogen; in BS 1016-7:1
10、977, clauses 5 and 6 and that part of clause 10 relating to carbon and hydrogen. Principal differences are that coal and coke are now considered together, the method follows a different procedure for conditioning the absorption train and the precision data has been revised. An alternative method is
11、given in Subsection 106.1.2 Liebig method. BS 1016-106 is part of a rationalized and restructured BS 1016. The Parts numbered from 1 to 21 are gradually being withdrawn and replaced by Parts in the new series. The full list of Parts in the new series, together with corresponding numbering of the old
12、 series and related international standards is given in BS 1016 Analysis and testing of coal and coke Part 100:1994 General introduction and methods for reporting results. The technical committee has reviewed the provisions of ISO 1015:1992, ISO 5068:1983 and ISO 5069-2:1983 to which normative refer
13、ence is made in the text, and has decided that they are acceptable for use in conjunction with this standard. British Standards related to ISO 331:1983, ISO 687:1974, ISO 925:1980 and ISO 1170:1977 are BS 1016 Methods for analysis and testing of coal and coke Section 104.1:1991 Determination of the
14、moisture content of the general analysis sample of coal, Section 104.2:1991 Determination of the moisture content of the general analysis sample of coke, Part 6:1991 Ultimate analysis of coal and Part 100:1994 General introduction and methods for reporting results respectively. British Standards rel
15、ated to ISO 1988:1975 and ISO 2309:1980 are BS 1017 Sampling of coal and coke Part 1:1989 Methods for sampling of coal and Part 2: 1994 Methods for sampling of coke. ISO 1988 and ISO 2309 are being revised and will be published in eight Parts, and it is intended to implement these parts as identical
16、 British Standards, superseding BS 1017. A British Standard does not purport to include all the necessary provisions of a contract. Users of British Standards are responsible for their correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations.
17、Summary of pages This document comprises a front cover, an inside front cover, pages i and ii, pages 1 to 10 and a back cover. This standard has been updated (see copyright date) and may have had amendments incorporated. This will be indicated in the amendment table on the inside front cover. Licens
18、ed Copy: sheffieldun sheffieldun, na, Fri Nov 24 08:07:58 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS 1016-106.1.1:1996 BSI 11-19981 Introduction An alternative method to that specified in this International Standard is given in ISO 625:1996, Solid mineral fuels Determination of carbon and hydroge
19、n Liebig method. 1 Scope This International Standard specifies a method of determining the total carbon and the total hydrogen in hard coal, brown coal and lignite, and coke, by a high temperature combustion method. The results include the carbon in the carbonates and the hydrogen combined in the mo
20、isture and in the water of constitution of silicates. A determination of moisture is carried out at the same time, and an appropriate correction is applied to the hydrogen value obtained by combustion. A determination of carbon dioxide may also be made and the total carbon value corrected for the pr
21、esence of mineral carbonates. 2 Normative references The following standards contain provisions which, through reference in this text, constitute provisions of this International Standard. At the time of publication, the editions indicated were valid. All standards are subject to revision, and parti
22、es to agreements based on this International Standard are encouraged to investigate the possibility of applying the most recent editions of the standards indicated below. Members of IEC and ISO maintain registers of currently valid International Standards. ISO 331:1983, Coal Determination of moistur
23、e in the analysis sample Direct gravimetric method. ISO 687:1974, Coke Determination of moisture in the analysis sample. ISO 925:1980, Solid mineral fuels Determination of carbon dioxide content Gravimetric method. ISO 1015:1992, Brown coals and lignites Determination of moisture content Direct volu
24、metric method. ISO 1170:1977, Coal and coke Calculation of analyses to different bases. ISO 1988:1975, Hard coal Sampling. ISO 2309:1980, Coke Sampling. ISO 5068:1983, Brown coals and lignites Determination of moisture content Indirect gravimetric method. ISO 5069-2:1983, Brown coals and lignites Pr
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