BS-EN-1948-3-2006.pdf
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1、BRITISH STANDARD BS EN 1948-3:2006 Stationary source emissions Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs Part 3: Identification and quantification of PCDDs/PCDFs The European Standard EN 1948-3:2006 has the status of a British Standard ICS 13.040.40 ? Licensed Copy:
2、 sheffieldun sheffieldun, na, Sun Oct 29 09:13:11 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS EN 1948-3:2006 This British Standard was published under the authority of the Standards Policy and Strategy Committee on 31 March 2006 BSI ISBN 0 580 48045 3 National foreword This British Standard is the
3、 official English language version of EN 1948-3:2006. It supersedes BS EN 1948-3:1997 which is withdrawn. The UK participation in its preparation was entrusted by Technical Committee EH/2, Air quality, to Subcommittee EH/2/1, Stationary source emissions, which has the responsibility to: A list of or
4、ganizations represented on this subcommittee can be obtained on request to its secretary. Cross-references The British Standards which implement international or European publications referred to in this document may be found in the BSI Catalogue under the section entitled “International Standards C
5、orrespondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard does
6、not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretation, or proposals for change, and keep UK interests informed; monitor related international and European development
7、s and promulgate them in the UK. Summary of pages This document comprises a front cover, an inside front cover, the EN title page, pages 2 to 48, an inside back cover and a back cover. The BSI copyright notice displayed in this document indicates when the document was last issued. Amendments issued
8、since publication Amd. No. DateComments Licensed Copy: sheffieldun sheffieldun, na, Sun Oct 29 09:13:11 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 1948-3 March 2006 ICS 13.040.40Supersedes EN 1948-3:1996 English Version Stationary source emissions
9、 - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs Emissions de sources fixes - Dtermination de la concentration massique en PCDD/PCDF et PCB de type dioxine - Partie 3: Identification et quantification de PCDD/PC
10、DF Emissionen aus stationren Quellen - Bestimmung der Massenkonzentration von PCDD/PCDF und dioxin- hnlichen PCB - Teil 3: Identifizierung und Quantifizierung von PCDD/PCDF This European Standard was approved by CEN on 23 January 2006. CEN members are bound to comply with the CEN/CENELEC Internal Re
11、gulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CEN member. This
12、 European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official versions. CEN members are the
13、 national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and Unite
14、d Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: rue de Stassart, 36 B-1050 Brussels 2006 CENAll rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 1948-3:2006:
15、 E Licensed Copy: sheffieldun sheffieldun, na, Sun Oct 29 09:13:11 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN 1948-3:2006 (E) 2 Contents Page Foreword 3 Introduction6 1 Scope.7 2 Normative references .7 3 Terms and definitions.7 4 Symbols and abbreviations10 5 Principles of identification and qua
16、ntification11 6 Reagents, materials and equipment11 7 Safety measures .11 8 Quality control requirements for identification and quantification.11 9 Quality assurance criteria for extraction/clean-up/quantification procedure blanks 13 10 Calibration of the HRGC/HRMS14 11 Quantification of HRGC/HRMS r
17、esults15 12 Calculation of the measurement results .18 13 Analytical report18 14 Performance characteristics19 15 Interferences .21 Annex A (informative) Examples of operation of gas chromatography / mass spectrometry analysis of PCDDs/PCDFs in emission samples22 Annex B (informative) Estimation of
18、the measuring uncertainty and precision of the determination of polychlorinated dibenzo-p-dioxins and dibenzofurans.31 Annex C (informative) Mass of ions monitored for PCDDs and PCDFs 35 Annex D (informative) Relative abundance of chlorine isotope ions and their ratio for PCDD/PCDF congeners contain
19、ing 4 to 8 chlorine substituents36 Annex E (informative) Further general recommendations for separation, detection and quantification of PCDDs/PCDFs 37 Annex F (informative) Variability determination based on the results of the validation tests.39 Annex G (informative) Relation to EU Directives 47 B
20、ibliography.48 Licensed Copy: sheffieldun sheffieldun, na, Sun Oct 29 09:13:11 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN 1948-3:2006 (E) 3 Foreword This European Standard (EN 1948-3:2006) has been prepared by Technical Committee CEN/TC 264 “Air quality”, the secretariat of which is held by DIN.
21、This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by September 2006, and conflicting national standards shall be withdrawn at the latest by September 2006. Attention is drawn to the possibility that so
22、me of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This European Standard supersedes EN 1948-3:1996. This European Standard has been prepared under a mandate given to CEN by the Euro
23、pean Commission and the European Free Trade Association to support Essential Requirements of EU Directive 94/67/EC of 16 December 1994 i on the incineration of hazardous waste. This directive is now replaced by EU Directive 2000/76/EC of 4 December 2000 on the incineration of waste ii and this Europ
24、ean Standard also supports the Essential Requirements of the new EU Directive 2000/76/EC (see also Annex G). The precision and the performance characteristics were determined between 1992 and 1995 in four comparative and validation trials at waste incinerators sponsored by the European Commission, t
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