BS-EN-15199-2-2006 BS-2000-507-2006.pdf
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1、BRITISH STANDARD BS EN 15199-2:2006 BS 2000-507: 2006 Petroleum products Determination of boiling range distribution by gas chromatography method Part 2: Heavy distillates and residual fuels The European Standard EN 15199-2:2006 has the status of a British Standard ICS 75.080 ? Licensed Copy: London
2、 South Bank University, London South Bank University, Thu Mar 01 08:55:41 GMT+00:00 2007, Uncontrolled Copy, (c) BSI BS EN 15199-2:2006 This British Standard was published under the authority of the Standards Policy and Strategy Committee on 31 January 2007 BSI and Energy Institute 2007 ISBN 978 0 5
3、80 50181 4 National foreword This British Standard was published by BSI. It is the UK implementation of EN 15199-2:2006. The UK participation in its preparation was entrusted to Technical Committee PTI/13, Petroleum testing and terminology. A list of organizations represented on PTI/13 can be obtain
4、ed on request to its secretary. Energy Institute, under the brand of IP, publishes and sells all Parts of BS 2000, and all BS EN petroleum test methods that would be Part of BS 2000, both in its annual publication “Standard methods for analysis and testing of petroleum and related products and Briti
5、sh Standard 2000 Parts” and individually. Further information is available from: Energy Institute, 61 New Cavendish Street, London W1G 7AR. Tel: 020 7467 7100. Fax: 020 7255 1472. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its c
6、orrect application. Compliance with a British Standard cannot confer immunity from legal obligations. Amendments issued since publication Amd. No. DateComments Licensed Copy: London South Bank University, London South Bank University, Thu Mar 01 08:55:41 GMT+00:00 2007, Uncontrolled Copy, (c) BSI EU
7、ROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 15199-2 October 2006 ICS 75.080 English Version Petroleum products - Determination of boiling range distribution by gas chromatography method - Part 2: Heavy distillates and residual fuels Produits ptroliers - Dtermination de la rpartition dans lint
8、ervalle de distillation par mthode chromatographie en phase gazeuse - Partie 2: Distillats severes et residuals Minerallerzeugnisse - Gaschromatographische Bestimmung des Siedeverlaufes - Teil 2: Schwerle und Rckstandsle This European Standard was approved by CEN on 28 August 2006. CEN members are b
9、ound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the
10、 Central Secretariat or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same statu
11、s as the official versions. CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia,
12、 Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: rue de Stassart, 36 B-1050 Brussels 2006 CENAll rights of exploitation in any form and by any means reserved worldwide for
13、 CEN national Members. Ref. No. EN 15199-2:2006: E Licensed Copy: London South Bank University, London South Bank University, Thu Mar 01 08:55:41 GMT+00:00 2007, Uncontrolled Copy, (c) BSI EN 15199-2:2006 (E) 2 Contents Page Foreword3 1 Scope 4 2 Normative references4 3 Terms and definitions .4 4 Pr
14、inciple6 5 Reagents and materials 6 6 Apparatus .9 7 Sampling procedure10 8 Preparation of the apparatus10 8.1 Gas chromatograph preparation10 8.2 System performance check10 9 Sample and reference material preparation10 10 Calibration11 11 Procedure .13 12 Visual inspection of the chromatograms13 13
15、 Calculation14 14 Expression of results 14 15 Precision.14 15.1 General14 15.2 Repeatability.14 15.3 Reproducibility.14 16 Test report15 Annex A (normative) Calculation procedure16 Annex B (normative) System performance check.19 Annex C (informative) Boiling points of normal alkanes 21 Annex D (info
16、rmative) Additional guidance for the calculation algorithm22 Bibliography26 Licensed Copy: London South Bank University, London South Bank University, Thu Mar 01 08:55:41 GMT+00:00 2007, Uncontrolled Copy, (c) BSI EN 15199-2:2006 (E) 3 Foreword This document (EN 15199-2:2006) has been prepared by Te
17、chnical Committee CEN/TC 19 “Gaseous and liquid fuels, lubricants and related products of petroleum, synthetic and biological origin”, the secretariat of which is held by NEN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by en
18、dorsement, at the latest by April 2007, and conflicting national standards shall be withdrawn at the latest by April 2007. EN 15199 consists of the following parts, under the general title Petroleum products Determination of boiling range distribution by gas chromatography method: Part 1: Middle dis
19、tillates and lubricating base oils Part 2: Heavy distillates and residual fuels Part 3: Crude oil This part of the standard describes the determination of boiling range distribution of materials with initial boiling points (IBP) above 100 C and final boiling points (FBP) above 750 C. For testing mat
20、erials with initial boiling points (IBP) above 100 C and final boiling point (FBP) below 750 C, Part 1 of the standard may be used. For testing materials with initial boiling points (IBP) below 100 C and final boiling points (FBP) above 750 C, such as crude oils, Part 3 is applicable. This part of t
21、he standard is a joint development between the EI 1, ASTM 2 and CEN. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland,
22、France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. Licensed Copy: London South Bank University, London South Bank University, Thu Mar 01 08
23、:55:41 GMT+00:00 2007, Uncontrolled Copy, (c) BSI EN 15199-2:2006 (E) 4 1 Scope This European Standard specifies a method for the determination of the boiling range distribution of petroleum products by capillary gas chromatography using flame ionisation detection. The standard is applicable to mate
24、rials having a vapour pressure low enough to permit sampling at ambient temperature, and which have a boiling range of at least 100 C. The standard is applicable to materials with initial boiling points (IBP) above 100 C and final boiling points (FBP) above 750 C, for example, heavy distillate fuels
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