《BS-ISO-21147-2003.pdf》由会员分享,可在线阅读,更多相关《BS-ISO-21147-2003.pdf(12页珍藏版)》请在三一文库上搜索。
1、BRITISH STANDARD BS ISO 21147:2003 Fine-cut tobacco and smoking articles made from it Survey and analysis of consumer-made articles ICS 65.160 ? Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 03:29:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS ISO 21147:2003 This British Standard was publ
2、ished under the authority of the Standards Policy and Strategy Committee on 5 March 2003 BSI 5 March 2003 ISBN 0 580 41347 0 National foreword This British Standard reproduces verbatim ISO 21147:2003 and implements it as the UK national standard. The UK participation in its preparation was entrusted
3、 to Technical Committee AW/40, Tobacco and tobacco products, which has the responsibility to: A list of organizations represented on this committee can be obtained on request to its secretary. Cross-references The British Standards which implement international publications referred to in this docum
4、ent may be found in the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online. This publication does not purport to include all the necessary provisions of a contract.
5、Users are responsible for its correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretation, or proposals for cha
6、nge, and keep the UK interests informed; monitor related international and European developments and promulgate them in the UK. Summary of pages This document comprises a front cover, an inside front cover, the ISO title page, pages ii to iv, pages 1 to 5 and a back cover. The BSI copyright date dis
7、played in this document indicates when the document was last issued. Amendments issued since publication Amd. No. DateComments Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 03:29:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI Reference number ISO 21147:2003(E) INTERNATIONAL STANDARD ISO 2114
8、7 First edition 2003-03-01 Fine-cut tobacco and smoking articles made from it Survey and analysis of consumer-made articles Tabac de fine coupe et objets confectionns partir de ce type de tabac Inventaire et analyse des objets confectionns par le consommateur BS ISO 21147:2003 Licensed Copy: sheffie
9、ldun sheffieldun, na, Mon Nov 27 03:29:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS ISO 21147:2003 ii Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 03:29:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI IS:74112 O3002(E) I SO 3002 All irhgts seredevr iii Foreword ISO (the International Org
10、anization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been establi
11、shed has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardizatio
12、n. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting.
13、Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such pat
14、ent rights. ISO 21147 was prepared by Technical Committee ISO/TC 126, Tobacco and tobacco products. BS ISO 21147:2003 iii Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 03:29:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI IS:74112 O3002(E) vi I SO 3002 All irhgts seredevr Introduction Studies
15、 to determine the nicotine-free dry particulate matter (NFDPM) and nicotine of smoking articles made by consumers have been reported in the literature (see Bibliography, references 1 and 2). The studies show that consumers make smoking articles that are extremely variable in terms of mass, diameter,
16、 density and size. The articles are frequently badly made and have very loosely filled ends. Great care must be taken when handling them. It is necessary that any study should ensure that the consumers chosen are experienced in hand-rolling smoking articles, that the number of smokers studied is lar
17、ge, and that the articles made are correctly sampled and carefully transported to the testing laboratory. The survey can be conducted either by providing tobacco and wrappers or the consumers can be asked to provide their own. Evidence in reference 3 shows that free tobacco provision leads to the us
18、e of more tobacco and higher smoke yields from the articles. On the other hand, non-provision leads to less well-controlled making conditions particularly with respect to tobacco moisture content. This factor is also known to affect article smoke yields. BS ISO 21147:2003 iv Licensed Copy: sheffield
19、un sheffieldun, na, Mon Nov 27 03:29:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI INTENRATIONAL TSANDADR IS:74112 O3002(E) I SO 3002 All irhgts seredevr 1 Fine-cut tobacco and smoking articles made from it Survey and analysis of consumer-made articles 1 Scope This International Standard specifies t
20、he method of conducing a survey to determine nicotine-free dry particulate matter and nicotine yields from fine-cut smoking articles made by consumers. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edi
21、tion cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 15592-2, Fine-cut tobacco and smoking articles made from it Methods of sampling, conditioning and analysis Part 2: Atmosphere for conditioning and testing ISO 15592-3:200
22、3, Fine-cut tobacco and smoking articles made from it Methods of sampling, conditioning and analysis Part 3: Determination of total particulate matter of smoking articles using a routine analytical smoking machine, preparation for the determination of water and nicotine, and calculation of nicotine-
23、free dry particulate matter 3 Terms, definitions and abbreviated terms For the purpose of this document, the following terms, definitions and abbreviated terms apply. 3.1 fine-cut tobacco FCT tobacco produced to be used by consumers for making their own smoking articles 3.2 fine-cut smoking article
24、FCSA article, suitable for smoking, produced by combining fine-cut tobacco with a wrapper 3.3 wrapper material specially prepared and supplied in a form suitable for enclosing fine-cut tobacco so as to produce a fine-cut smoking article 3.4 total particulate matter TPM that portion of the mainstream
25、 smoke which is retained in the smoke trap BS ISO 21147:2003 1 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 03:29:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI IS:74112 O3002(E) 2 I SO 3002 All irhgts seredevr 3.5 dry particulate matter DPM total particulate matter after deduction of its w
26、ater content 3.6 nicotine-free dry particulate matter NFDPM dry particulate matter after deduction of its nicotine content 4 Principle A panel of fine-cut tobacco consumers is selected. The panel members make fine-cut smoking articles (FCSAs). The samples are collected and packaged. The moisture con
27、tent, draw resistance, NFDPM and nicotine yields of the FCSAs are determined according to methods specified in ISO 15592-3. 5 Consumer panel selection Choose panel members from consumers who regularly make and smoke FCSAs at least once a day, preferably from the type of fine-cut tobacco and wrapper
28、being studied. Select the panel so that it is representative in socio-demographic terms and in quantity of tobacco used per week. A minimum panel size of 100 is required, but select a larger size if there is an intention to sub-classify the data. NOTE Pilot studies with a sample size of 40 may permi
29、t approximate findings. However, a study of 100 consumers is required to obtain satisfactory confidence limits. 6 Making FCSAs The Introduction discusses whether tobacco and wrappers should be supplied to the consumers. If they are to be supplied, then the tobacco to be used to make FCSAs shall be s
30、upplied at the moisture content at which it is normally sold. If the consumers are to supply their own tobacco and wrappers, they shall be asked to use their normal tobacco and wrappers. Each consumer shall be asked to make a minimum of 25 FCSAs and identify the intended mouth end. From these, 20 sa
31、mples shall be taken at random and used to determine smoke yields; two shall be used to determine the moisture content of the tobacco and the remainder shall be used to test draw resistance and to serve as spares in case of damage. For a more accurate determination, 45 samples shall be made to allow
32、 for two smoking runs of 20 FCSAs per consumer. NOTE Increasing the sample size to 45 may present a risk that the consumers would not take sufficient care over the making and consequently lead to FCSAs that are not truly representative. The consumers should ideally be asked to make the FCSAs in thei
33、r natural environment and by their normal manner of making. They should be required to make one for sampling and then a second one for smoking at the time when they wish to smoke until the number required for the study has been made. Sealable foam-lined containers shall be provided to protect and st
34、ore the FCSAs as they are made. BS ISO 21147:2003 2 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 03:29:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI IS:74112 O3002(E) I SO 3002 All irhgts seredevr 3 7 Laboratory analyses Condition the FCSAs according to ISO 15592-2, keeping separate those
35、made by each consumer. Inspect the FCSAs made by each consumer for physical defects. Defective FCSAs shall not be used for smoke analysis but can possibly be used to determine other properties. Identify each article for any subsequent reference without causing damage. Randomly select one FCSA per co
36、nsumer batch for determination of moisture content. Weigh and record the mass of each of 20 of the remaining FCSAs 40 if two smoking runs are to be made. Prepare and smoke the FCSAs according to 9.6 to 9.9.3 of ISO 15592-3:2003. Because of the nature of consumer-made FCSAs, it is most important that
37、 they are undamaged when inserted into the holders for smoking. Care should be taken to avoid leaks and it may be necessary to use sealant or a longer insertion depth to do so. If possible, measure the diameter of the remaining FCSAs at three places along the length. Measure to the nearest millimetr
38、e at places 10 mm from each end and in the middle. Express the result as the mean of the three measurements. Where possible, select the FCSA holder bobbin and latex sleeve dimensions appropriately (see ISO 15592-3:2003, 5.2). 8 Statistical evaluation Examine the data for statistical outliers. Take g
39、reat care to remove only those outliers arising from a known departure from procedure during the laboratory analysis because consumer-made articles are inherently very variable. 9 Test report 9.1 General The test report shall show the methods used and the results obtained. 9.2 Conduct of the survey
40、9.2.1 Tobacco and wrappers supplied The following particulars shall be included: a) type of tobacco; b) type of wrapper and its classification. 9.2.2 Tobacco and wrappers supplied by the consumers The following particulars shall be included: a) type of tobacco if not normal brand; b) type of wrapper
41、 and its classification. BS ISO 21147:2003 3 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 03:29:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI IS:74112 O3002(E) 4 I SO 3002 All irhgts seredevr 9.3 Consumer data The following data shall be reported: a) normal brands used of the fine-cut toba
42、cco and wrapper; b) daily consumption; c) whether other tobacco products are used and, if so, daily consumption; d) how the FCSAs were made (hand-rolled, making device, use of tubed wrapper, etc.); e) circumstances in which the FCSAs were made; f) date of receipt of the batch of FCSAs at the laborat
43、ory. 9.4 Laboratory data The following data shall be reported for each consumers batch of FCSAs: a) moisture content after conditioning, as mass fraction in percent to the nearest 0,1 %; b) tobacco mass of the individual fine-cut smoking articles, in milligrams to the nearest 1 mg; c) mean tobacco m
44、ass of the fine-cut smoking articles, in milligrams to the nearest 1 mg; d) diameter of the individual fine-cut smoking article, in millimetres to the nearest 0,5 mm; e) mean diameter of the fine-cut smoking articles, in millimetres to the nearest 0,1 mm; f) draw resistance of the individual fine-cu
45、t smoking articles, in pascals to the nearest 10 Pa; g) mean draw resistance of the fine-cut smoking articles, in pascals to the nearest 10 Pa; h) number of puffs; i) NFDPM yield, in milligrams to the nearest 1 mg; j) nicotine yield, in milligrams to the nearest 0,1 mg; k) type of smoking machine us
46、ed. 9.5 Statistical analysis Give a description of the methods of analysis used. BS ISO 21147:2003 4 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 03:29:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI IS:74112 O3002(E) I SO 3002 All irhgts seredevr 5 Bibliography 1 DYMOND, H.F. Making habit o
47、f roll-your-own smokers in The Netherlands and tar and nicotine yields from the resultant products. Tobacco Science, 40, 1996, pp. 87-91 2 DYMOND, H.F. Physical dimensions and tar and nicotine yields of fine-cut smoking articles rolled by German consumers. Beitr. z. Tabakforschung, 18 (4), 1999, pp.
48、 165-174 3 Report of the CORESTA Task Force on roll-your-own (fine-cut) tobacco. CORESTA Bulletin, 1999-2, Roll-your-own report BS ISO 21147:2003 5 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 03:29:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS ISO 21147:2003 BSI 389 Chiswick High Road
49、London W4 4AL BSI British Standards Institution BSI is the independent national body responsible for preparing British Standards. It presents the UK view on standards in Europe and at the international level. It is incorporated by Royal Charter. Revisions British Standards are updated by amendment or revision. Users of British Standards should make sure that they possess the latest amendments or editions. It is the constant aim of BSI to improve the quality of ou
链接地址:https://www.31doc.com/p-3747091.html