DD-CEN-TS-1071-7-2003.pdf
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1、DRAFT FOR DEVELOPMENT DD CEN/TS 1071-7:2003 Advanced technical ceramics Methods of test for ceramic coatings Part7: Determination of hardness and Youngs modulus by instrumented indentation testing ICS 81.060.30 ? Licensed Copy: London South Bank University, London South Bank University, Tue Dec 12 0
2、5:55:19 GMT+00:00 2006, Uncontrolled Copy, (c) BSI DD CEN/TS 1071-7:2003 This British Standard was published under the authority of the Standards Policy and Strategy Committee on 16 October 2003 BSI 16 October 2003 ISBN 0 580 42762 5 National foreword This Draft for Development is the official Engli
3、sh language version of DD CEN/TS 1071-7:2003. This publication is not to be regarded as a British Standard. It is being issued in the Draft for Development series of publications and is of a provisional nature because it is considered that further experience is required in its application before it
4、is converted to a European and hence British Standard. It should be applied on this provisional basis, so that information and experience of its practical application may be obtained. Comments arising from the use of this Draft for Development are requested so that UK experience can be reported to t
5、he European organization responsible for its conversion to a European Standard. A review of this publication will be initiated 2 years after its publication by the European organization so that a decision can be taken on its status at the end of its 3 year life. Notification of the start of the revi
6、ew period will be made in an announcement in the appropriate issue of Update Standards. According to the replies received by the end of the review period, the responsible BSI Committee will decide whether to support the conversion into a European Standard, to extend the life of the Technical Specifi
7、cation or to with draw it. Comments should be sent in writing to the Secretary of BSI Technical Committee RPI/13, Advance technical ceramics, at 389 Chiswick High Road, London W4 4AL, giving the document reference and clause number and proposing, where possible, an appropriate revision of the text.
8、A list of organizations represented on this committee can be obtained on request to its secretary. Cross-references The British Standards which implement international or European publications referred to in this document may be found in the BSI Catalogue under the section entitled “International St
9、andards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online. Summary of pages This document comprises a front cover, an inside front cover, the CEN/TS title page, pages 2 to 31 and a back cover. The BSI copyright date displayed in t
10、his document indicates when the document was last issued. Amendments issued since publication Amd. No. DateComments Licensed Copy: London South Bank University, London South Bank University, Tue Dec 12 05:55:19 GMT+00:00 2006, Uncontrolled Copy, (c) BSI TECHNICAL SPECIFICATION SPCIFICATION TECHNIQUE
11、 TECHNISCHE SPEZIFIKATION CEN/TS 1071-7 July 2003 ICS 81.060.30 English version Advanced technical ceramics - Methods of test for ceramic coatings - Part 7: Determination of hardness and Youngs modulus by instrumented indentation testing Hochleistungskeramik Verfahren zur Prfung keramischer Schichte
12、n Teil 7: Bestimmung der Hrte und des Elastizittsmoduls durch instrumentierte Eindringprfung Cramiques techniques avances Mthodes dessai pour revtements cramiques Partie 7: Dtermination de la duret et du module de Young par essai de pntration instrument This Technical Specification (CEN/TS) was appr
13、oved by CEN on 19 January 2003 for provisional application. The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to submit their comments, particularly on the question whether the CEN/TS can be converted into a European Stand
14、ard. CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS available. It is permissible to keep conflicting national standards in force (in parallel to the CEN/TS) until the final decision about the possible conversion of the CEN/TS int
15、o an EN is reached. CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMM
16、ITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: rue de Stassart, 36 B-1050 Brussels 2002 CENAll rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. CEN/TS 1071-7:2003 E Licensed Copy: Lon
17、don South Bank University, London South Bank University, Tue Dec 12 05:55:19 GMT+00:00 2006, Uncontrolled Copy, (c) BSI CEN/TS 1071-7:2003 (E) 2 ContentsPage Foreword. 3 Introduction 4 1Scope . 4 2Normative references . 4 3Terms and definitions. 5 4Apparatus and materials 6 5Preparation of test spec
18、imen. 7 5.1General. 7 5.2Surface roughness . 7 5.3Polishing 7 5.4Surface cleanliness 8 6Test procedure 8 6.1Calibration of instrument and indenters 8 6.2Test piece. 8 6.3Test conditions . 8 6.4Measurement. 9 7Data analysis and evaluation of results . 9 7.1Composite properties. 9 7.2Evaluation of coa
19、ting hardness and modulus from in-plan indentation data:. 10 8Test report . 11 Annex A (informative) Instrumented Indentation Testing (IIT) 16 A.1Principles of IIT . 16 A.2Instrument calibration procedures 17 A.2.1General. 17 A.2.2Force and displacement. 17 A.2.3Instrument frame stiffness and indent
20、er area function 17 A.3Determination of the zero point. 22 A.4Analysis Method . 24 A.4.1Introduction. 24 A.4.2Determination of contact depth. 24 Annex B (informative) Indenter cleaning procedure. 29 Bibliography. 30 Licensed Copy: London South Bank University, London South Bank University, Tue Dec 1
21、2 05:55:19 GMT+00:00 2006, Uncontrolled Copy, (c) BSI CEN/TS 1071-7:2003 (E) 3 Foreword This document (CEN/TS 1071-7:2003) has been prepared by Technical Committee CEN/TC 184 “Advanced technical ceramics”, the secretariat of which is held by BSI. This document has been prepared under a mandate given
22、 to CEN by the European Commission. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to announce this Technical Specification: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Hungary Iceland, Ire
23、land, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and the United Kingdom. EN 1071 Advanced technical ceramics - Methods of test for ceramic coatings consists of 11 Parts: Part 1:Determination of coating thickness by contact probe profilometer Part 2:
24、Determination of coating thickness by the crater grinding method Part 3:Determination of adhesion and other mechanical failure modes by a scratch test Part 4:Determination of chemical composition Part 5:Determination of porosity Part 6:Determination of the abrasion resistance of coatings by a micro-
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