ISO-20863-2004.pdf

Reference number ISO 20863:2004(E) © ISO 2004 INTERNATIONAL STANDARD ISO 20863 First edition 2004-12-01 Footwear Test methods for stiffeners and toepuffs Bondability Chaussures Méthodes d'essai pour contreforts et renforts Aptitude au collage Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=Aramco HQ/9980755100 Not for Resale, 04/23/2007 03:10:24 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 20863:2004(E) PDF disclaimer This PDF file may contain embedded typefaces. In accordance with Adobe's licensing policy, this file may be printed or viewed but shall not be edited unless the typefaces which are embedded are licensed to and installed on the computer performing the editing. In downloading this file, parties accept therein the responsibility of not infringing Adobe's licensing policy. The ISO Central Secretariat accepts no liability in this area. Adobe is a trademark of Adobe Systems Incorporated. Details of the software products used to create this PDF file can be found in the General Info relative to the file; the PDF-creation parameters were optimized for printing. Every care has been taken to ensure that the file is suitable for use by ISO member bodies. In the unlikely event that a problem relating to it is found, please inform the Central Secretariat at the address given below. © ISO 2004 All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means, electronic or mechanical, including photocopying and microfilm, without permission in writing from either ISO at the address below or ISO's member body in the country of the requester. ISO copyright office Case postale 56 CH-1211 Geneva 20 Tel. + 41 22 749 01 11 Fax + 41 22 749 09 47 E-mail copyrightiso.org Web www.iso.org Published in Switzerland ii © ISO 2004 All rights reserved Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=Aramco HQ/9980755100 Not for Resale, 04/23/2007 03:10:24 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 20863:2004(E) © ISO 2004 All rights reserved iii Foreword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 20863 was prepared by the European Committee for Standardization (CEN) in collaboration with Technical Committee ISO/TC 216, Footwear, in accordance with the Agreement on technical cooperation between ISO and CEN (Vienna Agreement). Throughout the text of this document, read “.this European Standard.” to mean “.this International Standard.”. Annex ZA provides a list of corresponding International and European Standards for which equivalents are not given in the text. Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=Aramco HQ/9980755100 Not for Resale, 04/23/2007 03:10:24 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 20863:2004(E) iv © ISO 2004 All rights reserved Contents Page Forewordv 1 Scope 1 2 Normative references 1 3 Terms and definitions .1 4 Apparatus and materials.1 5 Sampling and conditioning.2 5.1 Method 1: Heat activated materials2 5.2 Method 2: Solvent activated materials 2 6 Procedure .2 7 Expression of results 3 7.1 Dry bondability.3 7.2 Wet bondability 3 8 Test report 4 Annex ZA (normative) Normative references to International publications with their corresponding European publications5 Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=Aramco HQ/9980755100 Not for Resale, 04/23/2007 03:10:24 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 20863:2004(E) © ISO 2004 All rights reserved v Foreword This document (EN ISO 20863:2004) has been prepared by Technical Committee CEN/TC 309 “Footwear“, the secretariat of which is held by AENOR, in collaboration with Technical Committee ISO/TC 216 “Footwear“. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by June 2005, and conflicting national standards shall be withdrawn at the latest by June 2005. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=Aramco HQ/9980755100 Not for Resale, 04/23/2007 03:10:24 MDTNo reproduction or networking permitted without license from IHS -,-,- Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=Aramco HQ/9980755100 Not for Resale, 04/23/2007 03:10:24 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 20863:2004(E) © ISO 2004 All rights reserved 1 1 Scope This document specifies a method for the determination of the bondability of heat activated and solvent activated stiffeners and toepuffs to upper and lining materials. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 12222, Footwear Standard atmospheres for conditioning and testing of footwear and components for footwear. EN ISO 3696, Water for analytical laboratory use Specification and test methods (ISO 3696:1987). EN ISO 4048, Leather Determination of matter soluble in dichloromethane (ISO 4048:1977). EN ISO 7500-1, Metallic materials Verification of static uniaxial testing machines Part 1: Tension/compression testing machines Verification and calibration of the force-measuring system (ISO 7500-1:2004). 3 Terms and definitions For the purposes of this document, the following terms and definitions apply. bondability aptitude of a material to be bonded to it self or to other material by applying pressure and/or heat and eventually adhesive. 4 Apparatus and materials 4.1 General The following apparatus and materials shall be used. 4.2 Tensile testing machine with a jaw separation rate of 100 mm/min ± 10 mm/min, an appropriate force range (this will usually be less than 100 N), capable of measuring the force to an accuracy of better than 2 % as specified by class 2 in EN ISO 7500-1, which registers the force applied in terms of the displacement. 4.3 Press knife or other means of cutting rectangular test specimens of (150 mm ± 10mm) x (30 mm ± 2 mm). 4.4 Press with the following characteristics. 4.4.1 Heated plates which can maintain a pre-established temperature with a precision of ± 5 ºC. 4.4.2 Operating pressure of 245 kPa ± 5 kPa (245 kPa are 2,5 kg/cm2). 4.5 Reference leather, full chrome splits (thickness of 1,5 mm to 1,7 mm) with a grease content of 4 % in total fat and 1 % in fatty acid (see EN ISO 4048). 4.6 Non-woven fabric, 150 g ± 20 g per square metre. Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=Aramco HQ/9980755100 Not for Resale, 04/23/2007 03:10:24 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 20863:2004(E) 2 © ISO 2004 All rights reserved 4.7 Water distilled or deionised complying with grade 3 of EN ISO 3696. 5 Sampling and conditioning 5.1 Method 1: Heat activated materials 5.1.1 Cut sufficient strips of (150 mm ± 10 mm) x (30 mm ± 2 mm) from the sample and the corresponding strips of the same size from the non-woven fabric and the reference leather (4.5) or the material to be used. 5.1.2 Make a “compound test piece” of leather-sample-non-woven fabric. A strip of paper is placed on one of the short sides between the leather and the sample, so that 20 mm remain unstuck and so that the ends can be held in the jaws of the tensile testing machine. NOTE The side of the material to be tested should be that in contact with the standard leather, i.e. the side that in the shoe will be in contact with the upper leather. 5.1.3 Unless the manufacture establishes the application conditions, follow the Clauses 5.1.4 and 5.1.5. 5.1.4 Place the compound test piece between both press plates heated to 70 ºC ± 5 ºC, and apply a pressure of 245 kPa ± 5 kPa for 10 s. 5.1.5 Repeat the procedure described in sections 5.1.2 and 5.1.4 with the other test pieces and both press plates heated to 90 ºC ± 5 ºC, 110 ºC ± 5 ºC, 130 ºC ± 5 ºC and 150 ºC ± 5 ºC, respectively. 5.1.6 Condition the set test pieces in a conditioned environment as specified in EN 12222 for 24 h. 5.2 Method 2: Solvent activated materials 5.2.1 Cut at least two strips of (150 mm ± 10 mm) x (30 mm ± 2 mm) from the sample and two strips of the same size from the non-woven fabric and the reference leather (4.5) or the material to be used. 5.2.2 Activate the test specimen by applying acetone or other solvent (4.7) to it until it is uniformly wetted, then leave it for 2,5 min ± 0,5 min. 5.2.3 Make a “compound test piece” of leather-sample-non-woven fabric. A strip of paper is placed on one of the short sides between the leather and the sample, so that 20 mm remain unstuck and so that the ends can be held in the jaws of the tensile testing machine. 5.2.4 Unless the manufacturer establishes the application conditions, place the compound test piece between both press plates heated to 50 ºC ± 5 ºC, and apply a pressure of 245 kPa ± 5 kPa for 10 s (245 kPa are 2,5 kg/cm2). 5.2.5 Condition the set test pieces in a conditioned environment as specified in EN 12222 for 24 h. 6 Procedure 6.1 Fix the reference leather of the compound test piece in one of the jaws of the tensile testing machine and the end of the sample and the non-woven fabric in the other jaw. 6.2 Operate the tensile testing machine so that the jaw separates at a speed of 100 mm/min ± 10 mm/min. 6.3 Stop the tensile testing machine when half the length of the test piece has been unbonded. 6.4 Repeat the procedure described in 6.1, 6.2 and 6.3 with the other test pieces. Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=Aramco HQ/9980755100 Not for Resale, 04/23/2007 03:10:24 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 20863:2004(E) © ISO 2004 All rights reserved 3 6.5 Submerge the part of the test pieces which are still bonded, in distilled water for 16 h. 6.6 Remove a test piece from the water, hold the free ends of the wet test piece in the jaws of the tensile testing machine and unbond the rest of the test piece. 6.7 Repeat the procedure described in 6.6 with the other test pieces. 7 Expression of results 7.1 Dry bondability 7.1.1 Calculate the average value of force (see Figure 1) obtained for 6.3 and 6.4 for each one of the test pieces, in newtons. 7.1.2 Divide the average value of force obtained for each one of the test pieces by the width of the test piece, measured in millimetres, and express the dry bondability, in newtons per millimetre. Key 1 Force, in N 2 Average 3 Deformation Figure 1 Example of diagram force/deformation 7.2 Wet bondability 7.2.1 Calculate the average value of force obtained for 6.6 and 6.7 for each one of the wet test pieces, in newtons. 7.2.2 Divide the average value of force obtained in each one of the test pieces by the width of the test pieces, measured in millimetres, and express the wet bondability in newtons per millimetre. Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=Aramco HQ/9980755100 Not for Resale, 04/23/2007 03:10:24 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 20863:2004(E) 4 © ISO 2004 All rights reserved 8 Test report The test report shall include the following information: a) reference to this document; EN ISO 20863; b) a description of the samples tested, including commercial styles, codes, colours, nature, etc.; c) the average dry bondability or the average for each temperature tested as shown in 7.1; d) the average wet bondability or the average for each temperature tested as shown in 7.2; e) date of testing; f) any deviation from this standard test method. Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=Aramco HQ/9980755100 Not for Resale, 04/23/2007 03:10:24 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 20863:2004(E) © ISO 2004 All rights reserved 5 Annex ZA (normative) Normative references to International publications with their corresponding European publications The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. Publication Year Title EN Year ISO 3696 1987 Water for analytical laboratory use Specification and test methods. EN