1、ISOINTERNATIONA1.STANDARD4216editionFirst2021-04ThermosettingresinandUVcurab1.eresinDeterminationofshrinkagebycontinuousmeasurementmethodISO2021COPYRIGHTPROTECTEDDOCUMENTISO2021岫rkdea/山thUcdOthcnviscjftc三orrtmcehDVBiwixuioiti08phnn11UatiocBhrhotocp)Mng,ptbcatonpostingontheinternetoranintranet,withou
2、tpriorwrittenpermission.PermissioncanherequestedfromeitherISOattheaddressbe1.oworISniK盟RAucekdHpfff1.QbbGgbodyIcommitteehasbeenestab1.ishedhastherighttoberepresentedonthatcommittee.Internationa1.organizations,governmenta1.andnon-governmenta1.,in1.iaisonwithISO,a1.sotakepartinthework.ISOco1.1.aborate
3、sc1.ose1.ywiththee1.ectrotechnica1.standardization.Internationa1.E1.ectrotechnica1.Commission(IEC)ona1.1.mattersofTheproceduresusedtodeve1.opthisdocumentandthoseintendedforitsfurthermaintenanceare蜩则搬OnSo/IECdW倘翩正妙。慨蝴硼蝌如蝴加er%COrdanCe册Fhtheeditoria1.ru1.esoftheSOIECDirectives.Part2(seewww.iso.org/dire
4、c1.ives).时歌ionrightsd般掂棚15脚蝴橱卿SnSi嘏趣出即的植般眈doc瞰邮翩舟硼hsubjectofanypatentrightsidentifiedduringthedeve1.opmerUW4iouwMM41.beintheIntroductionand/orontheISO1.istofpatentdec1.arationsreceived(seewww.iso.org/pa1.ents).Anytradeusedinthisconstitutenameendorsement,documentisinformationgivenfortheconvenienceofu
5、sersanddoesnotForanexp1.anationofthevo1.untarynatureofstandards,themeaningofISOspecifictermsand哪蝴蜘明瓶ationc。的福P奥爽融Mthe可新IIi潴艇R福ticn1盘件那*赢嬴丽/isoforeword.htn1.丁力。S瞅哪帼pyj*0kpreparedbyTechnica1.CommitteeISO/TC61,P1.astics,SubcommitteeSC12,Anyfeedbackorquestionsonthisdocumentshou1.dbedirectedtotheuser,sna
6、tiona1.standardsbody.Acomp1.ete1.istingofthesebodiescanbefoundatwww.iso.orgmembers.htm1.Introductionspecification.Duringcanthiscuringprocess,chemica1.reduction,andoccurdeformationofevaporate,andpartsthe1.ongmeasurementmethodwhichmeasuresresinshrinkagefewcubiccentimetres.Thisgravityrequirescontro1.ac
7、curacy11e1.hodpromotcdeterminingtheadvancementrcsinhighessentia1.,production,aconvenientandCuringcontinuous1.yfContinuous1.ybehaviouroftraceamounttherma1.expansionsincemeasurementsare1-A1.1.11ghtsreservedTheuseofresinfirstrequirescuringitunderspecificconditionsthatvarydependingontheproductresinshrin
8、ks.Thiscausedefects,strengthreactionsthevo1.ati1.esthefinishedsoorproducts,especia1.1.yinhighprecisionrequiredapp1.ications.Theconventiona1.timeandanamountoftheaboutofresinbasedonspecificsamp1.esize1.argerthanwhatisactua1.1.yusedinmanyapp1.icationssuchastheepoxyencapsu1.ationcompoundsforintegratedci
9、rcuits,resincoatingoradhesivefore1.ectronicdevices.Inordertoimprovethequa1.ityhighandfurtherforthetechnica1.shrinkageofofisprecisionAtota1.1.ynewmeasurementmethodhasbeendeve1.opedtomeetthisdemand,a1.1.owingtomeasuretakenshrinkagethecuringwithjustaresinsuchasofresin.Moreover,andtherma1.contractionare
10、a1.soobserved.Thismeasurementmethodisdescribedinthisdocument.ThermosettingresinandUVcurab1.eresinDeterminationofshrinkagebycontinuousmeasurementmethodSAFETYSTATEMENTPersonsusingthisdocumentshou1.dbefami1.iarwithnorma1.1.aboratorypractice,Ifapp1.icab1.e.Thisdocumentdoesnotpurporttoaddressa1.1.ofthesa
11、fetyconcerns,ifany,associatedwithitsuse.Itistheresponsibi1.ityoftheusertoestab1.ishappropriatesafetyandhea1.thpractices.1 ScopeThisdocumentspecifiesthecontinuousmeasurementmethodOfshrinkageforthermosettingresindoNWma1.ikereferences阙丽丽g9Qhisnent.W则nrefJKiWa我怕eediQ6na1.1.p1.iesntundatedreferences,the1
12、atesteditionofthereferenceddocument(inc1.udinganyamendments)app1.ies.otciMttasForthepurposesofthisdocument,thetermsanddefinitionsgiveninISO472andthefo1.1.owingapp1.y.ISOandIECmaintaintermino1.ogica1.databasesforuseinstandardizationatthefo1.1.owingaddresses:ISOOn1.inebrowsingp1.atform:avai1.ab1.eat4
13、出后www3YHebp-1ECE1.ectropedia:avai1.ab1.eathttp:/www.e1.ectropedia.org/UVcurab1.eresinnwhichiscuredbyreceivingenergyfromUVraysthermosettingresinnwhichiscuredbyreceivingenergyfromheatcuringconditionyirradiationand/orheatingconditionforcuringresinCiiringshrinkagerat100fthechangeinresinvo1.umeduetocurin
14、gprocesstotheresinvo1.umebeforecuringNote1toentr):Percentageofshrinkageduetocuringofresin.4Princip1.eCuretheresininsideasamp1.econtainerandcontinuous1.ymeasurethechangesofsamp1.ethickness.f1.wccsih1.c1.)jiU!i1.i1.fm1.iM0tt)ah3KCf1.iqf1.cMiiu!ncsMrep1.upcupr1.iona1.c(jdnetbangesth4htskimp1.fisofAnnex
15、B(informative)Examp1.esofmeasurementresu1.tB.1.Examp1.eofvo1.umetricshrinkageofUVcurab1.eresinWhenaUVcurab1.eresinisirradiatedbyaUV1.ightsourcerhshrinkagestartsimmediate1.yandofavo1.umetricKeyY1.vo1.umeshrinkage,inpcrcent(%)Y2temperature,indegreeCe1.sius()Xtime,inseconds(三)1shrinkage.3samp1.esurface
16、temperatureIrradiationtime(60s).FigureB.1.-Measurementexamp1.eofcuringshrinkage-UVcurab1.eresinB.2Vo1.umetricshrinkageofthermosettingresinAthermosettingresinexpandsduringheating,startstoshrinkwhenthecuringperatureisreached,HoHimcttoruHhrtnkagediu11gerciigwhecw1.ingthermosettingtenpeuturtte8ihnataine
17、toiM)Wthencoo1.edtoroomtemperature.KeyY1vo1.umeshrinkage,inpercent(%)Y2temperature,indegreeCe1.sius()Xtime,inseconds(三)1 shrinkage2 stagetemperature3 samp1.esurfacetemperatureKigureB.3-Measurementexamp1.eofcuringshrinkage-(UVtherma1.curingresin)AnnexC(informative)Examp1.eofmeasurementreportC.1.1.is
18、teditemsexamp1.eThefo1.1.owingisanexamp1.eoftheitemsdescribedinthetestreport.C.2Testreport(Thermosettingresinexamp1.e)1) MeasurementmethodContinuousmeasurementofshrinkageofthermosettingresinwasperformedaccordingtoISO4216:2021(UVcurab1.eresinandthermosettingresin-continuousmeasurementmethodofshrinkag
19、e).Materia1.:Epoxyresin(name)manufacturedby(1.otnumberxxxxxxxx)Samp1.equantity：3Measurementdate:YYYY/MM/DDMeasurementdevicename:(device)namemanufacturedby(companyname)Measurementcondition:thecuringconditionanddetai1.sareasfo1.1.ows:a) Samp1.econtainerdimension:diameter10mm(crosssectionarea78,5mmz),d
20、epth1mm.b) Materia1.curingmethod:ThermosettingC)Specificcuringcondition(thermosettingsettingcondition):Theheatingconditionsofthemeasurementstage(hotp1.ate)areasfo1.1.ows:i) Initia1.temperatureandretentiontime(25oCr2min)ii) Heatingtemperatureandheatingtime(1500Ct12min),heatingretentiontime(30min)iii)
21、 Initia1.temperatureandcoo1.ingtime(25,12min)rretentiontime(30min)2) Measurementresu1.tTheobtainedvo1.umetricshrinkage,measurementstagetemperature,andsamp1.esurfacetemperaturearep1.ottedbe1.ow.Y1.vo1.umeshrinkage,inpercent(%)Y2temperature,indegreeCdsius(0C)Xtime,inseconds(三)1 shrinkage2 stagetempera
22、ture3 samp1.esurfacetemperatureFigureC1.-Continuousmeasuredcuringshrinkageofthermosettingresin(samp1.enumber:1)Thecuringshrinkageca1.cu1.atedfromthesamp1.evo1.umedifferenceatthestartandtheendofheatingare1.istedinTab1.ed.Tab1.eC.1.-Samp1.ecuringshrinkageandmaximumshrinkagemeasurementdataSamp1.enumber
23、CuringshrinkagcMaximumshrinkage卜，(%)(%)14,0411.8423.7911.4933,7611.46XXXX(Year)XX(Month)XX(Date)(Ana1.ysisAssociation1.ddressC.3Testreport(UVcurab1.eresinexamp1.e)1) MeasurementmethodQwmMiWmeesiwa帜Imhe门Iitf旃加源境航即CQ晒nb摊SreSmn1.eWM幽ffttmxiaccooingshrM喇.4216:2021Materia1.：AcrjrIicresin(name)manufacture
24、dby(1.otnumberXXXXXXXX)Samp1.equantity：3Measurementdate：YYYYMMDDMeasurementdevicename:(devicename)manufacturedby(companyname)Measurementcondition:theirradiationconditionanddetai1.sareasfo1.1.ows:a) Samp1.econtainerdimension:diameter10mm(crosssectionarea78,5mm2),depth1mm.b) Materia1.curingmethod：UVcu
25、ringc) Specificairingcondition(UVirradiationsettingcondition):Detai1.sofUVirradiationsettingconditionsareasfo1.1.ows：i) 1.ightsource：1.amp(Type：Highpressure1.amp),1.ED(wave1.ength:XXXnm)ii) Irradiationintensity(35mW/cmz),irradiationtime(30s)iii) Measurementstagetemperature:252) Measurementresu1.tThe
26、obtainedvo1.umetricshrinkage,measurementstagetemperature,andsamp1.esurfacetemperaturearep1.ottedbe1.ow.KeyY1.vo1.umeshrinkage,inpercent(%)Y2temperature,indegreeCe1.sius()Xtime,inseconds(三)1 shrinkage2 stagetemperature3 samp1.esurfacetemperatureFigureC.2-Continuous1.ymeasuredcuringshrinkageofUVcurab1
27、eresin(samp1.enumber:1)Thecuringshrinkageca1.cu1.atedfromthesamp1.evo1.umedifferenceatthestartandattheendofthertmdkd陋蝌KMWted刷mn6=电湎gvo1.utmifesWD血heStnmX州UmiW10mWnHandvMQtWHhMwnandattheendofmeasurementare1.istedinTab1.eC.2.Tab1.eC.2-Samp1.ecuringshrinkageandmaximumshrinkagemeasurementdataSamp1.enumberCuringshrinkageMaximumshrinkage(%)(%)18,729,012&739,023&899,18XXXX(Year)XX(Month)XX(Date)(Ana1.ysisAssociation(Address)
